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  • ASTM
    C758-18 Standard Test Methods for Chemical, Mass Spectrometric, Spectrochemical, Nuclear, and Radiochemical Analysis of Nuclear-Grade Plutonium Metal
    Edition: 2018
    $144.00
    Unlimited Users per year

Description of ASTM-C758 2018

ASTM C758-18

Active Standard: Standard Test Methods for Chemical, Mass Spectrometric, Spectrochemical, Nuclear, and Radiochemical Analysis of Nuclear-Grade Plutonium Metal




ASTM C758

Scope

1.1 These test methods cover procedures for the chemical, mass spectrometric, spectrochemical, nuclear, and radiochemical analysis of nuclear-grade plutonium metal to determine compliance with specifications.

1.2 The analytical procedures appear in the following order:

 

Sections

Dissolution Procedure

2

Plutonium by Controlled-Potential Coulometry

3

Plutonium by Amperometric Titration with Iron (II)

2

Plutonium by Ceric Sulfate Titration Test Method

3

Plutonium by Diode Array Spectrophotometry

3

Uranium by Arsenazo I Spectrophotometric Test Method

8 – 10

Thorium by Thorin Spectrophotometric Test Method

11 – 13

Iron by 1,10-Phenanthroline Spectrophotometric Test Method

14 – 16

Iron by 2,2ʹ-Bipyridyl Spectrophotometric Test Method

17 – 23

Impurities by ICP-AES

 

Chloride by the Thiocyanate Spectrophotometric Test Method

24 – 26

Fluoride by Distillation-Spectrophotometric Test Method

27–28

Nitrogen by Distillation-Nessler Reagent Spectrophotometric Test
 Method

29–30

Carbon by the Direct Combustion-Thermal Conductivity Test
 Method

31 – 33

Sulfur by Distillation-Spectrophotometric Test Method

34 – 36

Isotopic Composition by Mass Spectrometry

37 and 38

Plutonium-238 Isotopic Abundance by Alpha Spectrometry

 

Americium-241 by Extraction and Gamma Counting

39 – 41

Americium-241 by Gamma Counting

3

Gamma-Emitting Fission Products, Uranium, and Thorium by
 Gamma-Ray Spectroscopy

42 – 49

Rare Earths by Copper Spark Spectrochemical Test Method

50 – 52

Tungsten, Niobium (Columbium), and Tantalum by Spectro-
 chemical Test Method

53 – 55

Sample Preparation for Spectrographic Analysis for Trace Impuri-
 ties

56 – 60

1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific safeguard and safety hazards statements, see Section 6.

1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.


Keywords

impurity content; isotopic composition; plutonium content; plutonium metal;


ICS Code

ICS Number Code 27.120.30 (Fissile materials and nuclear fuel technology)


DOI: 10.1520/C0758-18



The following editions for this book are also available...

Format Year Publisher Type Title Annual Price
1998
ASTM
Model Standard
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2004
ASTM
Model Standard
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2010
ASTM
Model Standard
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2018
ASTM
Model Standard
 $144.00 Buy

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ASTM International, formerly known as the American Society for Testing and Materials (ASTM), is a globally recognized leader in the development and delivery of international voluntary consensus standards. Today, some 12,000 ASTM standards are used around the world to improve product quality, enhance safety, facilitate market access and trade, and build consumer confidence. ASTM’s leadership in international standards development is driven by the contributions of its members: more than 30,000 of the world’s top technical experts and business professionals representing 150 countries. Working in an open and transparent process and using ASTM’s advanced electronic infrastructure, ASTM members deliver the test methods, specifications, guides, and practices that support industries and governments worldwide.
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