1. Scope

1.1 This test method provides for the identification of certain resins, plasticizers, stabilizers, and fillers in poly(vinyl chloride) (PVC) compounds by an infrared spectrophotometric technique. In many cases, individual components may be measured quantitatively. Complementary procedures, such as chromatographic and other separations, will be necessary to separate specific components and extend the applications of this test method. Other instrumental test methods, such as optical emission or X-ray spectroscopic methods, may yield complementary information which may allow more complete or, in some cases, easier measurement of the components. The resin components covered in this test method are listed in the appendix.

1.2 PVC formulations are too varied to be covered adequately by a single test method. Using the following test method, many compounds may be separated into resins, plasticizers, stabilizers, and fillers. A number of components can be quantitatively measured. Many more can be identified and their concentrations estimated. By the use of prepared standards, one may determine the usefulness and accuracy of the test method for specific PVC formulations. This test method is applicable for the resin components listed in the appendix and for other components having similar chemical compositions and solubility characteristics. This test method can lead to error in cases where the nature of the components is not known.

1.3 The values stated in SI units are to be regarded as the standard. The values in parentheses are given for information only.

1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Note 1There is no similar or equivalent ISO standard.

2. Referenced Documents (purchase separately) The documents listed below are referenced within the subject standard but are not provided as part of the standard.

ASTM Standards

E131 Terminology Relating to Molecular Spectroscopy

E168 Practices for General Techniques of Infrared Quantitative Analysis

E177 Practice for Use of the Terms Precision and Bias in ASTM Test Methods

E275 Practice for Describing and Measuring Performance of Ultraviolet and Visible Spectrophotometers

Keywords

Composition analysis--plastics; Infrared (IR) analysis--plastics; Infrared spectroscopy; Poly(vinyl chloride)(PVC);

ICS Code

ICS Number Code 83.140.99 (Other rubber and plastic products)

DOI: 10.1520/D2124-99E01

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