ASTM D6010-96(2006)
Historical Standard: ASTM D6010-96(2006) Standard Practice for Closed Vessel Microwave Solvent Extraction of Organic Compounds from Solid Matrices
SUPERSEDED (see Active link, below)
ASTM D6010
1. Scope
1.1 This practice describes the closed vessel microwave extraction of soils, sediments, sludges, and wastes for subsequent determination of solvent extractable semivolatile and nonvolatile organic compounds by such techniques as gas chromatography and gas chromatography-mass spectrometry.
1.1.1 Compounds listed in Tables 1-5 can be extracted from the preceding materials.
1.2 This test method is applicable to samples that will pass through a 10-mesh (approximately 2-mm opening) screen.
1.3 The detection limit and linear concentration range for each compound is dependent on the gas chromatograph or gas chromatograph-mass spectrometer technique employed and may be found in the manual accompanying the instrument used.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. See Section for specific hazard statements.
2. Referenced Documents (purchase separately) The documents listed below are referenced within the subject standard but are not provided as part of the standard.
ASTM Standards
D1193 Specification for Reagent Water
D3976 Practice for Preparation of Sediment Samples for Chemical Analysis
D5368 Test Methods for Gravimetric Determination of Total Solvent Extractable Content (TSEC) of Solid Waste Samples
Keywords
extraction; microwave; organic compounds; safety; solvent; vessel ;
ICS Code
ICS Number Code 71.040.50 (Physicochemical methods of analysis)
DOI: 10.1520/D6010-96R06
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